allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside
CAS No.:152174-60-2
Molecular Formula:C₃₈H₃₀F₅NO₈S
Molecular Weight:755.716
Hs Code.:

Synonyms:allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

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Chemical Property of allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

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Technology Process of allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

There total 1 articles about allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.8%

: 89067-88-9
allyl-3,6-di-O-benzyl-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 135192-53-9
pentafluorophenoxythiocarbonyl chloride

: 152174-60-2
allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With dmap; In dichloromethane; for 14h; Ambient temperature;
DOI:10.1016/0008-6215(93)84087-M

Reference yield: 92.4%

: 152174-60-2
allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

: 152157-79-4
allyl 3,6-di-O-benzyl-2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 130 ℃; for 4h;
DOI:10.1016/0008-6215(93)84087-M

Reference yield:

: 152174-60-2
allyl 3,6-di-O-benzyl-2-deoxy-4-O-pentafluorophenoxythionocarbonyl-2-phthalimido-β-D-glucopyranoside

: 3,6-di-O-benzyl-2,4-dideoxy-2-phthalimido-α,β-D-xylo-hexopyranosyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 92.4 percent / tributyltin hydride, azobis(isobutyronitrile) (AIBN) / toluene / 4 h / 130 °C

2: 67.9 percent / PdCl₂, NaOAc / acetic acid; H₂O / 48 h / Ambient temperature

3: N,N-dimethyl(chloromethylene)ammonium chloride / CHCl₃ / 1 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); Vilsmeier reagent; tri-n-butyl-tin hydride; sodium acetate; palladium dichloride; In chloroform; water; acetic acid; toluene;
DOI:10.1016/0008-6215(93)84087-M