6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

Base Information

Chemical Name:6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol
CAS No.:463943-81-9
Molecular Formula:C₂₄H₃₂N₆O₁₄P₂
Molecular Weight:690.497
Hs Code.:

Synonyms:6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

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Chemical Property of 6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

Chemical Property:

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Technology Process of 6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

There total 6 articles about 6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 59618-80-3
adenosine monophosphate tri-n-butylammonium salt

: 463943-79-5
2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol-6-phosphate

: 463943-81-9
6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

Guidance literature:: adenosine monophosphate tri-n-butylammonium salt; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 25 ℃; for 2h;

2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol-6-phosphate; In N,N-dimethyl-formamide; at 25 ℃; for 48h;

With calf intestinal alkaline phosphatase; pH=7.45;
DOI:10.1139/v02-074

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 463943-81-9
6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / SnCl₄

2.1: NaBH₃(O₂CCF₃) / tetrahydrofuran / 18 h / 25 °C

3.1: 1.8 g / Et₃N / ethyl acetate / 3 h / 0 °C

4.1: 74 percent / K₂CO₃ / methanol / 25 °C

5.1: 69 percent / POCl₃; (EtO)3PO; H₂o / 0 - 4 °C

6.1: CDI / dimethylformamide / 2 h / 25 °C

6.2: dimethylformamide / 48 h / 25 °C

6.3: 64 percent / calf intestinal alkaline phosphatase / pH 7.45

With sodium (trifluoroacetoxy)borohydride; triethyl phosphate; water; tin(IV) chloride; potassium carbonate; triethylamine; 1,1'-carbonyldiimidazole; trichlorophosphate; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1139/v02-074

Reference yield:

: 23316-67-8
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl-1-carbonitrile

: 463943-81-9
6-adenosine-diphosphate-2,5-anhydro-1-deoxy-1-phenylacetamido-D-allitol

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaBH₃(O₂CCF₃) / tetrahydrofuran / 18 h / 25 °C

2.1: 1.8 g / Et₃N / ethyl acetate / 3 h / 0 °C

3.1: 74 percent / K₂CO₃ / methanol / 25 °C

4.1: 69 percent / POCl₃; (EtO)3PO; H₂o / 0 - 4 °C

5.1: CDI / dimethylformamide / 2 h / 25 °C

5.2: dimethylformamide / 48 h / 25 °C

5.3: 64 percent / calf intestinal alkaline phosphatase / pH 7.45

With sodium (trifluoroacetoxy)borohydride; triethyl phosphate; water; potassium carbonate; triethylamine; 1,1'-carbonyldiimidazole; trichlorophosphate; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1139/v02-074