4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

Base Information

Chemical Name:4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol
CAS No.:501668-71-9
Molecular Formula:C₃₁H₃₄N₂O
Molecular Weight:450.624
Hs Code.:

Synonyms:4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

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Chemical Property of 4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

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Technology Process of 4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

There total 3 articles about 4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 501668-70-8
(S)-2-Dibenzylamino-4-nitro-1,5-diphenyl-pentan-3-ol

: 501668-71-9
4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

Guidance literature:: With sodium tetrahydroborate; nickel dichloride; In methanol; at 0 ℃; for 0.333333h;
DOI:10.1021/jo026616j

Reference yield:

: 6125-24-2
2-Phenylnitroethane

: 501668-71-9
4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / TBAF*xH₂O / tetrahydrofuran / 0.33 h / 0 °C

2: 76 percent / NiCl₂*6H₂O; NaBH₄ / methanol / 0.33 h / 0 °C

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; nickel dichloride; In tetrahydrofuran; methanol; 1: Henry reaction;
DOI:10.1021/jo026616j

Reference yield:

: 123054-12-6,123808-74-2,136370-73-5,111060-64-1
(2S)-N,N-dibenzylphenylalaninal

: 501668-71-9
4-amino-2-N,N-dibenzylamino-1,5-diphenyl pentan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / TBAF*xH₂O / tetrahydrofuran / 0.33 h / 0 °C

2: 76 percent / NiCl₂*6H₂O; NaBH₄ / methanol / 0.33 h / 0 °C

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; nickel dichloride; In tetrahydrofuran; methanol; 1: Henry reaction;
DOI:10.1021/jo026616j