Technology Process of C35H48N7O7P
There total 6 articles about C35H48N7O7P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27H31N7O4; di-tert-butyl diisopropylphosphoramide;
With
1H-tetrazole;
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 1.33333h;
Inert atmosphere;
DOI:10.1039/c2cc33552b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium hydroxide / 1,4-dioxane / 0 - 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
3.1: 1H-tetrazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3.2: 1.33 h / 0 - 20 °C / Inert atmosphere
With
1H-tetrazole; ammonium hydroxide; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33552b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / -20 - 0 °C / Inert atmosphere
2.1: ammonium hydroxide / 1,4-dioxane / 0 - 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
4.1: 1H-tetrazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
4.2: 1.33 h / 0 - 20 °C / Inert atmosphere
With
1H-tetrazole; ammonium hydroxide; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33552b
