C₁₇H₁₈O₃Si

Base Information

• Chemical Name: C₁₇H₁₈O₃Si
• CAS No.: 1621098-05-2
• Molecular Formula: C₁₇H₁₈O₃Si
• Molecular Weight: 298.414
• Mol file: 1621098-05-2.mol

Synonyms:C₁₇H₁₈O₃Si

Chemical Property of C₁₇H₁₈O₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈O₃Si

There total 5 articles about C₁₇H₁₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C17H18O2Si → C17H18O3Si (1621098-05-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201402434

Reference yield:

C19H22O2Si (1621098-04-1) → C17H18O3Si (1621098-05-2)

Guidance literature:

Multi-step reaction with 3 steps

1: Grubbs catalyst first generation / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

2: dimethyl Isophthalate / acetonitrile / 28 h / 20 °C / Inert atmosphere; UV-irradiation

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

With Grubbs catalyst first generation; dimethyl Isophthalate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;

DOI:10.1002/chem.201402434

Reference yield:

cis-pent-2-ene-1,5-diol (27354-43-4) → C17H18O3Si (1621098-05-2)

Guidance literature:

Multi-step reaction with 3 steps

1: silver nitrate / N,N-dimethyl-formamide / 2.5 h / 0 °C / Inert atmosphere

2: dimethyl Isophthalate / acetonitrile / 28 h / 20 °C / Inert atmosphere; UV-irradiation

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

With dimethyl Isophthalate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/chem.201402434

upstream raw materials:

cis-pent-2-ene-1,5-diol

5,6-dihydro-pyran-2-one

C₁₉H₂₂O₂Si

Downstream raw materials:

C₁₉H₁₆Br₂O₅