1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

Base Information

Chemical Name:1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal
CAS No.:52041-27-7
Molecular Formula:C₂₄H₂₄O₆
Molecular Weight:408.451
Hs Code.:

Synonyms:1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

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Chemical Property of 1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

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Technology Process of 1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

There total 2 articles about 1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 1835-12-7
3-methoxy-4-benzyloxy-α-bromoacetophenone

: 52041-27-7
1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 2h;
DOI:10.1016/S0040-4020(97)00460-2

Reference yield:

: 1835-11-6
4-benzyloxy-3-methoxyacetophenone

: 52041-27-7
1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / Br₂ / CHCl₃; CCl₄ / 1) 5 deg C, 20 min, 2) 5 deg C -> 40 deg C, 2 h

2: 95 percent / K₂CO₃ / dimethylformamide / 2 h / 25 °C

With bromine; potassium carbonate; In tetrachloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00460-2

Reference yield:

: 52041-27-7
1-(3'-methoxy-4'-(1-phenyl)methoxyphenyl)-2-(2'',6''-dimethoxyphenoxy)ethanal

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; methanol / 3 h / 20 °C

2: lithium tetrafluoroborate / N,N-dimethyl-formamide / 2.5 h / 20 °C / Electrolysis

With methanol; lithium tetrafluoroborate; palladium 10% on activated carbon; In N,N-dimethyl-formamide;
DOI:10.1039/d0gc03597a