Piperazine, 1-(10,11-dihydrodibenzo(a,d)cyclohepten-5-yl)-

Base Information

• Chemical Name: Piperazine, 1-(10,11-dihydrodibenzo(a,d)cyclohepten-5-yl)-
• CAS No.: 69159-50-8
• Molecular Formula: C19H22N2
• Molecular Weight: 278.397
• Hs Code.: 2933599090
• European Community (EC) Number: 671-435-7
• DSSTox Substance ID: DTXSID80219214
• Nikkaji Number: J1.809.541F
• Wikidata: Q83096130
• ChEMBL ID: CHEMBL1193950
• Mol file: 69159-50-8.mol

Synonyms:1-(10,11-dihydro-5H-dibenzo(a,d)cyclohepten-5-yl)piperazine;dibenzosuberanylpiperazine

Chemical Property of Piperazine, 1-(10,11-dihydrodibenzo(a,d)cyclohepten-5-yl)-

Chemical Property:

• Vapor Pressure: 1.06E-06mmHg at 25°C
• Melting Point: 105-107°C
• Refractive Index: 1.604
• Boiling Point: 402.9 °C at 760 mmHg
• Flash Point: 154.7 °C
• PSA: 15.27000
• Density: 1.109 g/cm³
• LogP: 3.04650
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 278.178298710
• Heavy Atom Count: 21
• Complexity: 313

Purity/Quality:

98%min ^*data from raw suppliers

1-(Dibenzosuberyl)piperazine 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2=CC=CC=C2C(C3=CC=CC=C31)N4CCNCC4

Technology Process of Piperazine, 1-(10,11-dihydrodibenzo(a,d)cyclohepten-5-yl)-

There total 7 articles about Piperazine, 1-(10,11-dihydrodibenzo(a,d)cyclohepten-5-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

piperazine (110-85-0) + 5-chlorodibenzosuberane (1210-33-9) → 1-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazine (69159-50-8)

Guidance literature:

In 1,4-dioxane; for 7h; Heating;

DOI:10.1021/jm960869l

Reference yield:

di-isopropyl ether (108-20-3) + 5-chlorodibenzosuberane (1210-33-9) → 1-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazine (69159-50-8)

Guidance literature:

In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

dibenzosuberol (1210-34-0) → 1-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazine (69159-50-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 93 percent / CaCl₂, HCl / benzene / 2.5 h

2: 80 percent / K₂CO₃ / CHCl₃ / Heating

3: KOH / ethanol / Heating

With hydrogenchloride; potassium hydroxide; potassium carbonate; calcium chloride; In ethanol; chloroform; benzene;

upstream raw materials:

piperazine

5-chlorodibenzosuberane

1-(ethoxycarbonyl)-4-(10,11-dihydro-5H-dibenzocycloheptene-5-yl)piperazine

dibenzosuberol

Downstream raw materials:

MS 073

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