phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Base Information

• Chemical Name: phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate
• CAS No.: 260430-51-1
• Molecular Formula: C₃₀H₃₂N₂O₄
• Molecular Weight: 484.595
• Mol file: 260430-51-1.mol

Synonyms:phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Chemical Property of phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

There total 2 articles about phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C30H34N2O4 → phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate (260430-51-1)

Guidance literature:

With copper(I) trifluoromethanesolfonate toluene complex; In dichloromethane; acetonitrile; at 20 ℃; for 1h;

DOI:10.1002/ejoc.201600246

Reference yield: 41.0%

phenylmethyl 4-({1-[(tert-butyl)oxycarbonyl]indol-2-yl}ethylidene)-3-ethylidenepiperidine-1-carboxylate (261895-13-0) → phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate (260430-51-1)

Guidance literature:

In benzene; Irradiation;

DOI:10.3987/COM-99-8759

Reference yield: 88.0%

phenylmethyl 6-[(tert-butyl)oxycarbonyl]-5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate (260430-51-1) → phenylmethyl 5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate (187614-65-9)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.3987/COM-99-8759

upstream raw materials:

phenylmethyl 4-({1-[(tert-butyl)oxycarbonyl]indol-2-yl}ethylidene)-3-ethylidenepiperidine-1-carboxylate

Downstream raw materials:

phenylmethyl 5,11-dimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

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