C₃₂H₄₄O₃Si

Base Information

Chemical Name:C₃₂H₄₄O₃Si
CAS No.:1374425-33-8
Molecular Formula:C₃₂H₄₄O₃Si
Molecular Weight:504.785
Hs Code.:

C<sub>32</sub>H<sub>44</sub>O<sub>3</sub>Si

Synonyms:C₃₂H₄₄O₃Si

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Chemical Property of C₃₂H₄₄O₃Si

Chemical Property:

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Technology Process of C₃₂H₄₄O₃Si

There total 17 articles about C₃₂H₄₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1374425-31-6
C₃₂H₄₂O₃Si

: 1374425-33-8
C₃₂H₄₄O₃Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/ejoc.201101629

Reference yield:

: C₁₃H₂₀O₅

: 1374425-33-8
C₃₂H₄₄O₃Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

5.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

6.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

7.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

7.3: 5 h / -78 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

9.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 °C / Inert atmosphere

10.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; iodine; oxygen; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629

Reference yield:

: 1374425-20-3
C₁₃H₂₀O₃

: 1374425-33-8
C₃₂H₄₄O₃Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: ozone / dichloromethane / 3 h / -78 °C

2.2: 4 h / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

7.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

8.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

9.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

9.3: 5 h / -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

11.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

12.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; n-butyllithium; dihydrogen peroxide; iodine; oxygen; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629