4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

Base Information

Chemical Name:4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid
CAS No.:1104381-03-4
Molecular Formula:C₁₅H₂₀BF₃O₅
Molecular Weight:348.127
Hs Code.:

Synonyms:4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

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Chemical Property of 4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

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Technology Process of 4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

There total 3 articles about 4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5419-55-6
Triisopropyl borate

: 1104381-02-3
2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran

: 1104381-03-4
4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

Guidance literature:: 2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.216667h;

Triisopropyl borate; In tetrahydrofuran; at -78 - 20 ℃; for 0.883333h;

With acetic acid; In tetrahydrofuran;

Reference yield:

: 1104381-02-3
2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran

: 1104381-03-4
4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

Guidance literature:: 2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With acetic acid; In tetrahydrofuran; water;

Reference yield:

: 1104381-02-3
2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran

: 1104381-03-4
4-(3-(tetrahydro-2H-pyran-2-yloxy)-propoxy)-3-(trifluoromethyl)-phenylboronic acid

: C₃₀H₃₆B₂F₆O₈

: C₄₅H₅₄B₃F₉O₁₂

Guidance literature:: 2-[3-(4-bromo-2-(trifluoromethyl)-phenoxy)-propoxy]-tetrahydro-2H-pyran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.216667h;

With Triisopropyl borate; In tetrahydrofuran; at -78 - 20 ℃; for 0.883333h;

With water; acetic acid; In tetrahydrofuran;