1,8-bis(ferrocenyl)naphthalene

Base Information

Chemical Name:1,8-bis(ferrocenyl)naphthalene
CAS No.:94161-70-3
Molecular Formula:C₃₀H₂₄Fe₂
Molecular Weight:496.215
Hs Code.:

Synonyms:1,8-bis(ferrocenyl)naphthalene

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Chemical Property of 1,8-bis(ferrocenyl)naphthalene

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Technology Process of 1,8-bis(ferrocenyl)naphthalene

There total 4 articles about 1,8-bis(ferrocenyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: ferrocenylzinc(II) chloride

: 1730-04-7
1,8-diiodonaphthalene

: 91-20-3,71998-51-1,72931-45-4
naphthalene

: α-naphthylferrocene

: 94161-70-3
1,8-bis(ferrocenyl)naphthalene

Guidance literature:: [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In tetrahydrofuran; (N2), THF soln. of the complex added to a soln. of 5 mol% of the catalyst and the org. compd. in THF at 0°C, warmed to room temp., stirred for 3 h, refluxed for 1 h; quenched with 10% HCl, extd. with 3 portions of ether, combined extractwashed with water, dried over MgSO4, solvent removed, sepd. on silica gel plates using 10% CH2Cl2 in hexane;
DOI:10.1021/om00122a019

Reference yield: 52.0%

: ferrocenylzinc(II) chloride

: 17135-74-9
1,8-dibromonaphthalene

: 91-20-3,71998-51-1,72931-45-4
naphthalene

: α-naphthylferrocene

: 94161-70-3
1,8-bis(ferrocenyl)naphthalene

Guidance literature:: tetrakis(triphenylphosphine)nickel⁽⁰⁾; In tetrahydrofuran; (N2), org. compd. added to 5 mol% of catalyst in THF, stirred for 30 min at 0°C, soln. of the complex in THF added, stiiring at 0°C continued for 1 h, warmed to room temp., stirred overnight; quenched with 10% HCl, extd. with 3 portions of ether, combined extractwashed with water, dried over MgSO4, solvent removed, sepd. on silica gel plates using 10% CH2Cl2 in hexane, elem. anal.;
DOI:10.1021/om00122a019

Reference yield: 49.0%

: ferrocenylmagnesium bromide

: 1730-04-7
1,8-diiodonaphthalene

: 91-20-3,71998-51-1,72931-45-4
naphthalene

: α-naphthylferrocene

: 94161-70-3
1,8-bis(ferrocenyl)naphthalene

Guidance literature:: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In tetrahydrofuran; (N2), 5 mol% of catalyst and org. compd. stirred for 30 min in THF, complex in THF added at 0°C, stirred overnight at room temp.; quenched with 10% HCl, extd. with 3 portions of ether, combined extractwashed with water, dried over MgSO4, solvent removed, sepd. on silica gel plates using 10% CH2Cl2 in hexane;
DOI:10.1021/om00122a019