2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

Base Information

Chemical Name:2',3'-dideoxy-E-5-styryluridine 5'-monophosphate
CAS No.:158358-52-2
Molecular Formula:C₁₇H₁₉N₂O₇P
Molecular Weight:394.321
Hs Code.:

Synonyms:2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

Chemical Property:

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Technology Process of 2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

There total 1 articles about 2',3'-dideoxy-E-5-styryluridine 5'-monophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2',3'-dideoxy-E-5-styryluridine

: 158358-52-2
2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

Guidance literature:: With triethyl phosphate; trichlorophosphate; at 0 - 4 ℃; for 15h;
DOI:10.1080/15257779408012149

Reference yield:

: 158358-52-2
2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

: 2',3'-dideoxy-5-(2-phenethyl)uridine 5'-triphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-carbonyldiimidazole, tri-n-butylammonium pyrophosphate / 1.) DMF, RT, 5 h, 2.) RT, 15 h

2: 55 percent / H₂ / Pd/C / H₂O / 20 h / Ambient temperature

With hydrogen; tri(n-butyl)ammonium pyrophosphate; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In water;
DOI:10.1080/15257779408012149

Reference yield:

: 158358-52-2
2',3'-dideoxy-E-5-styryluridine 5'-monophosphate

: 147163-22-2
2',3'-dideoxy-E-5-styryluridine 5'-triphosphate

Guidance literature:: With tri(n-butyl)ammonium pyrophosphate; 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) DMF, RT, 5 h, 2.) RT, 15 h;
DOI:10.1080/15257779408012149