C₂₆H₂₆N₆S₄

Base Information

• Chemical Name: C₂₆H₂₆N₆S₄
• CAS No.: 132807-03-5
• Molecular Formula: C₂₆H₂₆N₆S₄
• Molecular Weight: 550.797
• Mol file: 132807-03-5.mol

Synonyms:C₂₆H₂₆N₆S₄

Chemical Property of C₂₆H₂₆N₆S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₆N₆S₄

There total 4 articles about C₂₆H₂₆N₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

Propyl isocyanate (110-78-1) + 4-phenyl-3-triphenylphosphoranylidenaminothiazole-2(3H)-thione (132834-48-1) → C26H26N6S4 (132807-03-5)

Guidance literature:

In dichloromethane; for 16h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97029-1

Reference yield: 41.0%

Propyl isocyanate (110-78-1) + 4-phenyl-3-triphenylphosphoranylidenaminothiazole-2(3H)-thione (132834-48-1) → C26H26N6S4 (132807-03-5)

Guidance literature:

In dichloromethane; for 16h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90791-4

Reference yield:

3-amino-4-phenylthiazoline-2(3H)-thione (5316-81-4) → C26H26N6S4 (132807-03-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Br₂, 2.) triethylamine / 1. a) benzene, 0-5 deg C, 1 h, b) up to r.t., 2.) benzene, reflux, 16 h

2: 41 percent / CH₂Cl₂ / 16 h / Ambient temperature

With bromine; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(01)90791-4

upstream raw materials:

Propyl isocyanate

4-phenyl-3-triphenylphosphoranylidenaminothiazole-2(3H)-thione

3-amino-4-phenylthiazoline-2(3H)-thione

Refernces

• 1、 Molina, Pedro,Arques, Antonio,Alias, Asuncion,Velasco, Maria D.. "Synthesis and electrochemical properties of the unknown N,N-bisheteroaryl amines bearing a fused heterocycle as N-substituent". . p. 6219 - 6222. Retrieved 2007/12/18.