(2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile

Base Information

Chemical Name:(2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile
CAS No.:3695-94-1
Molecular Formula:C₁₅H₉Cl₂N
Molecular Weight:274.149
Hs Code.:
European Community (EC) Number:666-190-8
NSC Number:287554
Mol file:3695-94-1.mol

Synonyms:(2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile;NSC287554;3695-94-1;NSC-287554;STK294390;AKOS000369529;4-CHLORO-ALPHA-(4-CHLOROPHENYL)CINNAMONITRILE

Suppliers and Price of (2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile

Chemical Property:

Vapor Pressure:1.09E-06mmHg at 25°C
Boiling Point:402.5°C at 760 mmHg
Flash Point:166.2°C
Density:1.306g/cm³
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:273.0112047
Heavy Atom Count:18
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C=C(C#N)C2=CC=C(C=C2)Cl)Cl
Isomeric SMILES:C1=CC(=CC=C1/C=C(/C#N)\C2=CC=C(C=C2)Cl)Cl

Technology Process of (2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile

There total 2 articles about (2E)-2,3-bis(4-chlorophenyl)prop-2-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 104-88-1
4-chlorobenzaldehyde

: 140-53-4
p-chlorobenzyl cyanide

: 70777-66-1,3695-94-1
1,2-Bis-(4-chlor-phenyl)-1-cyan-ethylen

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 6h;
DOI:10.1055/s-0032-1317351

Reference yield: 82.0%

: 70777-66-1,3695-94-1
1,2-Bis-(4-chlor-phenyl)-1-cyan-ethylen

Guidance literature:: With nickel(II) chloride hexahydrate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; zinc; In water; acetonitrile; at 80 ℃; for 10h; Glovebox; Inert atmosphere;

Reference yield: 93.0%

: 70777-66-1,3695-94-1
1,2-Bis-(4-chlor-phenyl)-1-cyan-ethylen

: C₁₈H₂₆N₂O₄

: ethyl 4-((2R,3R,4R,5R)-3,4-bis(4-chlorophenyl)-4-cyano-5-neopentylpyrrolidine-2-carboxamido)-3-methoxybenzoate

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; C₃₃H₃₀FeNOP; caesium carbonate; In tetrahydrofuran; at -40 ℃; for 0.5h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/cjoc.201900530