1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole

Base Information

Chemical Name:1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole
CAS No.:95552-66-2
Molecular Formula:C₂₈H₂₆Zr
Molecular Weight:453.738
Hs Code.:

Synonyms:1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole

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Technology Process of 1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole

There total 3 articles about 1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.3%

: [(Me-cyclopentadienyl)2Zr(H)(μ-H)]2

: 536-74-3
phenylacetylene

: 95552-66-2
1,1-bis(η5-methylcyclopentadienyl)-2,5-diphenylzirconole

Guidance literature:: In tetrahydrofuran; byproducts: H2; under N2 or Ar, PhCCH added to a suspn. of Zr-compd., at 23°C for 41 h and at 35°C for 54.5 h; volatiles removed in vac. at 45°C, dissolved in benzene, filtered, chromy. of the filtrate with benzene, evepd., extd. with CH2Cl2, evapd., crystd. after several days at room temp., washed with pentane, elem.anal., hydrolysis;