Technology Process of C40H58N4O6P2
There total 3 articles about C40H58N4O6P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine;
In
dichloromethane;
for 20h;
Inert atmosphere;
DOI:10.1021/om300409y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide / tetrahydrofuran; methanol / 5 h / 50 °C / Inert atmosphere; Schlenk technique
2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 20 h / Inert atmosphere
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/om300409y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / ethanol / 22 h / 65 °C / Inert atmosphere; Schlenk technique
2: lithium hydroxide / tetrahydrofuran; methanol / 5 h / 50 °C / Inert atmosphere; Schlenk technique
3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 20 h / Inert atmosphere
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/om300409y