1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene

Base Information

• Chemical Name: 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene
• CAS No.: 527698-52-8
• Molecular Formula: C₂₆H₄₉I₃SSi₃
• Molecular Weight: 858.711
• Mol file: 527698-52-8.mol

Synonyms:1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene

Chemical Property of 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene

There total 2 articles about 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene (527698-51-7) → 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene (527698-52-8)

Guidance literature:

With sodium iodide; In butanone; at 80 ℃; for 24h;

DOI:10.1039/b210358n

Reference yield:

1-(1,1-diallyl-but-3-enyl)-4-methylsulfanyl-benzene (289699-82-7) → 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene (527698-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 48 h / 20 °C

2: 85 percent / NaI / butan-2-one / 24 h / 80 °C

With sodium iodide; In diethyl ether; butanone;

DOI:10.1039/b210358n

Reference yield: 60.0%

4-triallylmethylphenol (224191-80-4) + 1-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene (527698-52-8) → C74H106O3SSi3

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 48h;

DOI:10.1039/b210358n

upstream raw materials:

1-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-4-methylsulfanyl-benzene

1-(1,1-diallyl-but-3-enyl)-4-methylsulfanyl-benzene