methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

Base Information

Chemical Name:methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate
CAS No.:1616960-11-2
Molecular Formula:C₂₅H₂₄N₂O₄
Molecular Weight:416.477
Hs Code.:

Synonyms:methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

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Chemical Property of methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

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Technology Process of methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

There total 3 articles about methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1357477-68-9
methyl 6-(6-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

: 62-53-3
aniline

: 1616960-11-2
methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 40 ℃; for 24h;
DOI:10.1016/j.dyepig.2014.05.006

Reference yield:

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 1616960-11-2
methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 0.75 h / 100 °C / Microwave irradiation

2: caesium carbonate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 24 h / 40 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In ethanol; toluene; 2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.dyepig.2014.05.006

Reference yield:

: 1926-80-3
methyl 6-aminocaproate hydrochloride

: 1616960-11-2
methyl 6-(1,3-dioxo-6-(phenylamino)-1H-benzo[de]isoquinolin-2(3H)-yl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 0.75 h / 100 °C / Microwave irradiation

2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate / 24 h / 40 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In ethanol; 2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.ejmech.2018.11.020