(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

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Chemical Name:(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene
CAS No.:143345-13-5
Molecular Formula:C₂₉H₃₇N₃O₃
Molecular Weight:475.631
Hs Code.:

Synonyms:(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

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Chemical Property of (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

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Technology Process of (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

There total 7 articles about (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 112633-26-8
2,6-bis[(tosyloxy)methyl]pyridine

: 143331-37-7
(3S,13S)-(+)-3,13-diphenyl-2,14-diaza-5,8,11-trioxapentadecane

: 143345-13-5
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

Guidance literature:: With sodium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1021/jo00046a020

Reference yield: 52.0%

: 143331-33-3
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dithione

: 143345-13-5
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

Guidance literature:: With nickel; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1021/jo00046a020

Reference yield:

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 143345-13-5
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / triethylamine / toluene / 24 h / Ambient temperature

2: 90 percent / Lawesson's reagent / toluene / 9 h / Heating

3: 52 percent / Raney nickel / tetrahydrofuran / 12 h / Ambient temperature

With Lawessons reagent; nickel; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jo00046a020