(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

Base Information

Chemical Name:(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane
CAS No.:1372610-45-1
Molecular Formula:C₂₆H₃₈N₂O₂
Molecular Weight:410.6
Hs Code.:

Synonyms:(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

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Chemical Property of (1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

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Technology Process of (1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

There total 5 articles about (1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 65838-10-0,135613-88-6,143443-23-6,191480-61-2
(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine

: 16088-62-3
(S)-Propylene oxide

: 1372610-45-1
(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

Guidance literature:: In methanol; at 40 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1007/s10562-012-0814-4

Reference yield:

: 3187-82-4,65838-45-1,113282-15-8,135682-70-1,147127-11-5,133695-15-5
(R,R)-N,N′-bis(phenylmethylene)-1,2-cyclohexanediamine

: 1372610-45-1
(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / 0.25 h / 20 °C / Reflux

2: methanol / 24 h / 40 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol;
DOI:10.1007/s10562-012-0814-4

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 1372610-45-1
(1R,2R)-N,N'-dibenzyl-N,N'-bis(ethan-(1-(S)-methyl)-1-ol)-trans-diaminocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0.53 h / 20 °C / Reflux; Inert atmosphere

2: sodium tetrahydroborate / 0.25 h / 20 °C / Reflux

3: methanol / 24 h / 40 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol;
DOI:10.1007/s10562-012-0814-4