C₂₇H₃₃NO₅S

Base Information

Chemical Name:C₂₇H₃₃NO₅S
CAS No.:1443437-11-3
Molecular Formula:C₂₇H₃₃NO₅S
Molecular Weight:483.629
Hs Code.:

C<sub>27</sub>H<sub>33</sub>NO<sub>5</sub>S

Synonyms:C₂₇H₃₃NO₅S

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Chemical Property of C₂₇H₃₃NO₅S

Chemical Property:

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Technology Process of C₂₇H₃₃NO₅S

There total 18 articles about C₂₇H₃₃NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1443437-10-2
(6S,8S)-tert-butyl 4-ethyl-7,8-dihydro-6-(hydroxymethyl)-8-methylcyclopenta[g]indole-1(6H)-carboxylate

: 98-59-9
p-toluenesulfonyl chloride

: 1443437-11-3
C₂₇H₃₃NO₅S

Guidance literature:: With pyridine; triethylamine; In dichloromethane; at 20 ℃; for 21h;
DOI:10.1002/chem.201202413

Reference yield:

: 161988-90-5
7-bromo-4-ethyl-1H-indole

: 1443437-11-3
C₂₇H₃₃NO₅S

Guidance literature:: Multi-step reaction with 15 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h

1.2: 12 h / 20 °C

2.1: palladium dichloride; triethylamine; tris-(o-tolyl)phosphine / acetonitrile / 15 h / 110 °C / Schlenk technique; Inert atmosphere

3.1: magnesium; methanol / 13 h / Reflux

4.1: Amano lipase PS-IM (immobilized on diatomaceous earth) / water; di-isopropyl ether / 65 h / 40 °C / Resolution of racemate; Enzymatic reaction

5.1: copper(I) bromide dimethylsulfide complex; methanol / diethyl ether / 5 h / 0 - 20 °C / Reflux

6.1: pyridine; dmap / dichloromethane / 13 h / 20 °C

7.1: dimethyl sulfoxide / 10 h / 60 °C

8.1: ethylene glycol; potassium hydroxide / water / 12 h / 110 °C

9.1: trifluoroacetic acid; trifluoroacetic anhydride / 0.08 h / 0 °C

10.1: aluminum (III) chloride; methoxybenzene / 3 h / 100 °C

11.1: dmap / dichloromethane / 3 h / Schlenk technique

12.1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C / Schlenk technique

13.1: phosphoric acid / N,N-dimethyl-formamide / 4.5 h / 80 - 100 °C / Schlenk technique

14.1: thallium(III) nitrate trihydrate / acetonitrile / 0.08 h / -40 °C / Schlenk technique; Inert atmosphere

14.2: 0.33 h / -20 °C

15.1: pyridine; triethylamine / dichloromethane / 21 h / 20 °C

With pyridine; methanol; dmap; aluminum (III) chloride; sodium tetrahydroborate; copper(I) bromide dimethylsulfide complex; thallium(III) nitrate trihydrate; phosphoric acid; Amano lipase PS-IM (immobilized on diatomaceous earth); magnesium; ethylene glycol; methoxybenzene; triethylamine; tris-(o-tolyl)phosphine; trifluoroacetic acid; trifluoroacetic anhydride; potassium hydroxide; palladium dichloride; In methanol; diethyl ether; dichloromethane; di-isopropyl ether; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201202413

Reference yield:

: C₂₀H₂₇NO₂

: 1443437-11-3
C₂₇H₃₃NO₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoric acid / N,N-dimethyl-formamide / 4.5 h / 80 - 100 °C / Schlenk technique

2.1: thallium(III) nitrate trihydrate / acetonitrile / 0.08 h / -40 °C / Schlenk technique; Inert atmosphere

2.2: 0.33 h / -20 °C

3.1: pyridine; triethylamine / dichloromethane / 21 h / 20 °C

With pyridine; thallium(III) nitrate trihydrate; phosphoric acid; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201202413