6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

Base Information

Chemical Name:6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid
CAS No.:77239-73-7
Molecular Formula:C₁₆H₁₇N₃O₂
Molecular Weight:283.33
Hs Code.:

Synonyms:6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

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Chemical Property of 6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

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Technology Process of 6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

There total 3 articles about 6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 77239-68-0
3-(2',4'-Dimethylphenyl)-6-cyano-5-oxo-cyclohex-3-ene-1-carboxylic acid

: 77239-73-7
6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Heating;

Reference yield:

: 132972-06-6,132972-07-7,22660-11-3
β-(2,4-dimethyl)benzoyl acrylic acid

: 77239-73-7
6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaOMe / 10 h / 170 °C

2: 65 percent / NaOMe / 10 h / 170 °C

3: 80 percent / N₂H₄*H₂O / ethanol / 6 h / Heating

With sodium methylate; hydrazine hydrate; In ethanol;

Reference yield:

: 77239-53-3
2-[2-(2,4-Dimethyl-phenyl)-2-oxo-ethyl]-3-ethoxycarbonyl-succinic acid 4-ethyl ester

: 77239-73-7
6-Cyano-3-(2,4-dimethyl-phenyl)-5-hydrazono-cyclohex-3-enecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOMe / 10 h / 170 °C

2: 80 percent / N₂H₄*H₂O / ethanol / 6 h / Heating

With sodium methylate; hydrazine hydrate; In ethanol;