[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester
CAS No.:948038-78-6
Molecular Formula:C₁₈H₂₆Cl₂N₂O₂
Molecular Weight:373.323
Hs Code.:

Synonyms:[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

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Chemical Property of [1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of [1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

There total 1 articles about [1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73874-95-0,179110-74-8
tert-butyl N-(piperidin-4-yl)carbamate hydrochloride

: 948038-77-5
3,4-dichloro-2-methyl-benzaldehyde

: 948038-78-6
[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

Guidance literature:: tert-butyl N-(piperidin-4-yl)carbamate hydrochloride; 3,4-dichloro-2-methyl-benzaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In tetrahydrofuran; at 20 ℃;

With water; sodium hydrogencarbonate; In tetrahydrofuran;

Reference yield:

: 948038-78-6
[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

: 1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-ylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 948038-78-6
[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-carbamic acid tert-butyl ester

: 948038-80-0
2-chloro-N-[1-(3,4-dichloro-2-methyl-benzyl)-piperidin-4-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 1 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;