1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

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Chemical Name:1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid
CAS No.:1403387-99-4
Molecular Formula:C₂₆H₃₉NO₃S
Molecular Weight:445.667
Hs Code.:

Synonyms:1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

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Chemical Property of 1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

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Technology Process of 1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

There total 3 articles about 1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1403387-98-3
1-(cyclohexylmethyl)-2-(3,5-di-tert-butylphenyl)-5-methyl-1H-pyrrole

: 1403387-99-4
1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

Guidance literature:: 1-(cyclohexylmethyl)-2-(3,5-di-tert-butylphenyl)-5-methyl-1H-pyrrole; With chlorosulfonic acid; In tetrahydrofuran; at -78 ℃; for 3h;

With water; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 1403387-99-4
1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 75 - 80 °C

2: toluene-4-sulfonic acid / toluene / 20 h / Reflux

3: chlorosulfonic acid / tetrahydrofuran / 3 h / -78 °C

With chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; toluene;

Reference yield:

: 1269473-15-5
1-(3,5-di-tert-butylphenyl)pentane-1,4-dione

: 1403387-99-4
1-(cyclohexylmethyl)-5-(3,5-di-tert-butylphenyl)-2-methyl-1H-pyrrole-3-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 20 h / Reflux

2: chlorosulfonic acid / tetrahydrofuran / 3 h / -78 °C

With chlorosulfonic acid; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;