Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

Base Information

Chemical Name:Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester
CAS No.:103681-11-4
Molecular Formula:C₁₈H₂₇ClO₂SSi
Molecular Weight:371.016
Hs Code.:

Synonyms:Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

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Chemical Property of Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

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Technology Process of Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

There total 9 articles about Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59376-64-6
(2E)-3-(trimethylsilyl)prop-2-en-1-ol

: 103681-11-4
Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / Pyridine / tetrahydrofuran / 0 °C

2: 1.) Zn / THF, HMPA

3: 2.) H₂O, H⁽¹⁺⁾ / 2.) heating

4: LiAlH₄

6: carbon homologation

7: Ph₃P, Diethyl azodicarboxylate

With pyridine; lithium aluminium tetrahydride; water; hydrogen cation; triphenylphosphine; zinc; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)98900-7

Reference yield:

: 103-04-8
(phenylthio)acetic acid

: 103681-11-4
Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-Chlorosuccinimide / CCl₄ / 0.83 h / 40 °C

2: Ph₃P, Diethyl azodicarboxylate

With N-chloro-succinimide; triphenylphosphine; diethylazodicarboxylate; In tetrachloromethane;
DOI:10.1016/S0040-4039(00)98900-7

Reference yield:

: 103681-21-6
3-Trimethylsilanyl-pent-4-en-1-ol

: 103681-11-4
Chloro-phenylsulfanyl-acetic acid 5-trimethylsilanyl-hept-6-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: carbon homologation

3: Ph₃P, Diethyl azodicarboxylate

With triphenylphosphine; diethylazodicarboxylate;
DOI:10.1016/S0040-4039(00)98900-7