methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate
CAS No.:1158804-09-1
Molecular Formula:C₁₅H₁₇N₃O₄
Molecular Weight:303.318
Hs Code.:

Synonyms:methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

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Chemical Property of methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

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Technology Process of methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

There total 4 articles about methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1158804-08-0
methyl 3-methoxy-4-(2-(ethoxycarbonyl)-3-oxobutyl)benzoate

: 124-46-9,20734-13-8,100224-74-6,593-85-1,90332-86-8,3425-08-9
guanidine hydrogen carbonate

: 1158804-09-1
methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

Guidance literature:: In methanol; at 65 ℃; for 16h;

Reference yield:

: 1158804-08-0
methyl 3-methoxy-4-(2-(ethoxycarbonyl)-3-oxobutyl)benzoate

: 593-85-1,90332-86-8,3425-08-9
diguanidine carbonate

: 1158804-09-1
methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

Guidance literature:: In ethanol; at 80 ℃; for 15h;

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 1158804-09-1
methyl 4-((2-amino-4-hydroxy-6-methylpyrimidin-5-yl)methyl)-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

1.2: 15 h / 70 °C

1.3: 0.5 h / Cooling with ice

2.1: ethanol / 15 h / 80 °C

With sodium hydride; In tetrahydrofuran; ethanol; mineral oil;