(2Z,4E)-methyl heptadeca-2,4-dienoate

Base Information

Chemical Name:(2Z,4E)-methyl heptadeca-2,4-dienoate
CAS No.:910452-46-9
Molecular Formula:C₁₈H₃₂O₂
Molecular Weight:280.451
Hs Code.:

Synonyms:(2Z,4E)-methyl heptadeca-2,4-dienoate

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Chemical Property of (2Z,4E)-methyl heptadeca-2,4-dienoate

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Technology Process of (2Z,4E)-methyl heptadeca-2,4-dienoate

There total 1 articles about (2Z,4E)-methyl heptadeca-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6064-48-8
1-hydroxy-2(E)-pentadecene

: 910452-46-9
(2Z,4E)-methyl heptadeca-2,4-dienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / MnO₂ / hexane / 24 h / 20 °C

2: 93 percent / 18-crown-6; t-BuOK / tetrahydrofuran / 2.5 h / -78 °C

With manganese(IV) oxide; 18-crown-6 ether; potassium tert-butylate; In tetrahydrofuran; hexane; 2: Still-Gennari reaction;
DOI:10.1021/jo061057s

Reference yield:

: 910452-46-9
(2Z,4E)-methyl heptadeca-2,4-dienoate

: (R)-1'-((S)-5''-oxo-tetrahydrofuran-2''-yl)tridecyl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: OsO₄; MeSO₂NH₂; (DHQ)2PHAL / K₃Fe(CN)6; K₂CO₃ / 2-methyl-propan-2-ol; H₂O / 0 °C

2: 97 percent / H₂ / Pd/C / methanol / 24 h / 760 Torr

3: 92 percent / PPh₃; DEAD / tetrahydrofuran / 2 h / 20 °C

With osmium(VIII) oxide; Hydroquinone 1,4-phthalazinediyl diether; methanesulfonamide; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; water; tert-butyl alcohol; 1: Sharpless asymmetric dihydroxylation / 3: Mitsunobu reaction;
DOI:10.1021/jo061057s