diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

Base Information

Chemical Name:diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside
CAS No.:484002-06-4
Molecular Formula:C₆₃H₇₆O₁₇
Molecular Weight:1105.29
Hs Code.:

Synonyms:diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

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Chemical Property of diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

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Technology Process of diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

There total 6 articles about diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14144-06-0
trillin

: 484002-06-4
diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: p-TsOH / dimethylformamide / 50 °C / pH 3 - 4

2: pyridine

3: 72 percent / p-TsOH / methanol; CH₂Cl₂ / Heating

4: 73 percent / TMSOTf / CH₂Cl₂ / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo026103c

Reference yield:

: 120969-06-4
diosgenyl 2,3,4,6-O-tetra-benzoyl-β-D-glucuronopyranoside

: 484002-06-4
diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: NaOMe / methanol; CH₂Cl₂ / 20 °C

2: p-TsOH / dimethylformamide / 50 °C / pH 3 - 4

3: pyridine

4: 72 percent / p-TsOH / methanol; CH₂Cl₂ / Heating

5: 73 percent / TMSOTf / CH₂Cl₂ / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo026103c

Reference yield:

: 211797-89-6
diosgenyl 4,6-O-benzylidene-β-D-glucopyranoside

: 484002-06-4
diosgenin-3-yl 2,3-di-O-acetyl-6-O-(2,3,4-tri-O-benzoyl-L-arabpyranosyl)-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: 72 percent / p-TsOH / methanol; CH₂Cl₂ / Heating

3: 73 percent / TMSOTf / CH₂Cl₂ / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1021/jo026103c