Technology Process of C34H39FN4O6S
There total 7 articles about C34H39FN4O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
DMF (N,N-dimethyl-formamide);
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Burgess Reagent / 1,2-dichloro-ethane / 0.25 h / 80 °C / Microwave
2.1: lithium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C
2.2: 20 °C
3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
With
lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C
1.2: 20 °C
2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
With
lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide);