phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside
CAS No.:1363661-34-0
Molecular Formula:C₁₈H₂₆O₁₀S
Molecular Weight:436.465
Hs Code.:

Synonyms:phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

There total 9 articles about phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1363661-32-8
phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 1363661-34-0
phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 5h;

In methanol; for 0.25h;
DOI:10.1021/ja208564y

Reference yield:

: C₃₁H₃₇F₃O₁₇⁽¹⁸⁾OS₂

: 1363661-34-0
phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite / N,N-dimethyl-formamide / 50 °C

2.1: pyridine / dichloromethane / 4 h / 0 - 20 °C

3.1: 2,6-dimethylpyridine; water / tetrahydrofuran / 1 h / 40 °C

4.1: sodium methylate / methanol / 5 h / 20 °C

4.2: Amberlite IR-120+ resin(H⁺form) / 0.25 h

With pyridine; 2,6-dimethylpyridine; water; sodium methylate; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja208564y

Reference yield:

: 1363661-30-6
phenyl (2,6-di-O-acetyl-4-O-(18)O-acetyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 1363661-34-0
phenyl ((3-(18)O)-β-D-(3-(18)O)galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 4 h / 0 - 20 °C

2.1: 2,6-dimethylpyridine; water / tetrahydrofuran / 1 h / 40 °C

3.1: sodium methylate / methanol / 5 h / 20 °C

3.2: Amberlite IR-120+ resin(H⁺form) / 0.25 h

With pyridine; 2,6-dimethylpyridine; water; sodium methylate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja208564y