[2,3,4-⁽¹³⁾C₃]daidzein

Base Information

Chemical Name:[2,3,4-⁽¹³⁾C₃]daidzein
CAS No.:1229516-23-7
Molecular Formula:C₁₅H₁₀O₄
Molecular Weight:257.209
Hs Code.:

[2,3,4-<sup>(13)</sup>C<sub>3</sub>]daidzein

Synonyms:[2,3,4-⁽¹³⁾C₃]daidzein

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2,3,4-⁽¹³⁾C₃]daidzein

Chemical Property:

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Technology Process of [2,3,4-⁽¹³⁾C₃]daidzein

There total 3 articles about [2,3,4-⁽¹³⁾C₃]daidzein which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)-3,3-dimethoxy-1-[1,2,3-⁽¹³⁾C₃]propanone

: 1229516-23-7
[2,3,4-⁽¹³⁾C₃]daidzein

Guidance literature:: With hydrogenchloride; water; In methanol; Reflux;
DOI:10.1002/jlcr.1732

Reference yield:

: 2-(4-benzyloxyphenyl)-1-(2,4-bis(benzyloxy)phenyl)-3,3-dimethoxy-1-[1,2,3-⁽¹³⁾C₃]propanone

: 1229516-23-7
[2,3,4-⁽¹³⁾C₃]daidzein

Guidance literature:: Multi-step reaction with 2 steps

1: 5% Pd(II)/C(eggshell); hydrogen / methanol; acetone / 20 °C

2: hydrogenchloride; water / methanol / Reflux

With hydrogenchloride; 5% Pd(II)/C(eggshell); water; hydrogen; In methanol; acetone;
DOI:10.1002/jlcr.1732

Reference yield:

: 74291-78-4
2,4-dihydroxy-[1',2'-⁽¹³⁾C₂]acetophenone

: 1229516-23-7
[2,3,4-⁽¹³⁾C₃]daidzein

Guidance literature:: Multi-step reaction with 5 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 8 h / Reflux

2: potassium hydroxide / ethanol / 5 h / Inert atmosphere; Reflux

3: thallium(III) nitrate trihydrate / methanol / 20 °C

4: 5% Pd(II)/C(eggshell); hydrogen / methanol; acetone / 20 °C

5: hydrogenchloride; water / methanol / Reflux

With hydrogenchloride; thallium(III) nitrate trihydrate; 18-crown-6 ether; 5% Pd(II)/C(eggshell); water; hydrogen; potassium carbonate; potassium hydroxide; In methanol; ethanol; acetone;
DOI:10.1002/jlcr.1732