N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

Base Information

Chemical Name:N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride
CAS No.:1350629-91-2
Molecular Formula:C₁₈H₂₇N₄O₂*Cl
Molecular Weight:366.891
Hs Code.:

Synonyms:N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

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Chemical Property of N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

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Technology Process of N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

There total 4 articles about N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1332315-16-8
4-[4-(chloromethyl)phenyl]-1,2-dimethyl-5-nitro-1H-imidazole

: 121-44-8
triethylamine

: 1350629-91-2
N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

Guidance literature:: In acetone; at 44 ℃; for 24h;
DOI:10.1016/j.tetlet.2011.10.096

Reference yield:

: 1197836-54-6
[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)phenyl]methanol

: 1350629-91-2
N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 16 h / 20 °C

2: acetone / 24 h / 44 °C

With thionyl chloride; In acetone;
DOI:10.1016/j.tetlet.2011.10.096

Reference yield:

: 59016-93-2
p-hydroxymethylphenylboronic acid

: 1350629-91-2
N-[4-(1,2-dimethyl-5-nitro-1H-imidazol-4-yl)benzyl]-N,N-diethylethanaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; ethanol / 0.5 h / Microwave irradiation

2: thionyl chloride / 16 h / 20 °C

3: acetone / 24 h / 44 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium carbonate; In 1,2-dimethoxyethane; ethanol; acetone; 1: Suzuki-Miyaura coupling;
DOI:10.1016/j.tetlet.2011.10.096