3-(benzyloxymethoxy)glutaric anhydride

Base Information

Chemical Name:3-(benzyloxymethoxy)glutaric anhydride
CAS No.:1607830-32-9
Molecular Formula:C₁₃H₁₄O₅
Molecular Weight:250.251
Hs Code.:

Synonyms:3-(benzyloxymethoxy)glutaric anhydride

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Chemical Property of 3-(benzyloxymethoxy)glutaric anhydride

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Technology Process of 3-(benzyloxymethoxy)glutaric anhydride

There total 4 articles about 3-(benzyloxymethoxy)glutaric anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1607830-31-8
3-(benzyloxymethoxy)glutaric acid

: 1607830-32-9
3-(benzyloxymethoxy)glutaric anhydride

Guidance literature:: In acetic anhydride; at 100 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/ejoc.201301374

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 1607830-32-9
3-(benzyloxymethoxy)glutaric anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / dichloromethane / 20 °C / Inert atmosphere

2: lithium hydrochloride monohydrate / methanol; water / 4 h / 20 °C / Inert atmosphere

3: acetic anhydride / 1.5 h / 100 °C / Inert atmosphere

With lithium hydrochloride monohydrate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water; acetic anhydride;
DOI:10.1002/ejoc.201301374

Reference yield:

: 1607830-30-7
diethyl 3-(benzyloxymethyloxy)glutarate

: 1607830-32-9
3-(benzyloxymethoxy)glutaric anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydrochloride monohydrate / methanol; water / 4 h / 20 °C / Inert atmosphere

2: acetic anhydride / 1.5 h / 100 °C / Inert atmosphere

With lithium hydrochloride monohydrate; In methanol; water; acetic anhydride;
DOI:10.1002/ejoc.201301374