2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

Base Information

Chemical Name:2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl
CAS No.:124190-07-4
Molecular Formula:C₁₈H₁₆N₅O₁₁
Molecular Weight:478.352
Hs Code.:

Synonyms:2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

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Chemical Property of 2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

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Technology Process of 2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

There total 6 articles about 2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 124190-06-3,147814-27-5
2,5-dimethyl-trans-2,5-di(3-nitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

: 124190-07-4
2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

Guidance literature:: With sulfuric acid; nitric acid; In water; at 0 ℃; for 0.5h;

Reference yield:

: 28765-36-8
2,5-dimethyl-3,4-dihydro-2H-pyrrole 1-oxide

: 124190-07-4
2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) O₂, 25percent aq. NH₄OH, Cu(OAc)2 / 1.) ether; 2.) MeOH, 30min

2: 62 percent / diethyl ether / 6 h / Ambient temperature

3: 63 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

4: 72 percent / 50percent aq. NaOH / dioxane / 3 h / Heating

5: 80 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

With ammonium hydroxide; sodium hydroxide; copper diacetate; sulfuric acid; oxygen; nitric acid; In 1,4-dioxane; diethyl ether; water;

Reference yield:

: 124189-88-4
trans-2,5-di(4-fluorophenyl)-2,5-dimethylpyrrolidin-1-oxyl

: 124190-07-4
2,5-dimethyl-trans-2,5-di(3,5-dinitro-4-hydroxyphenyl)pyrrolidin-1-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

2: 72 percent / 50percent aq. NaOH / dioxane / 3 h / Heating

3: 80 percent / conc. H₂SO₄, 67percent HNO₃ / H₂O / 0.5 h / 0 °C

With sodium hydroxide; sulfuric acid; nitric acid; In 1,4-dioxane; water;