4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Base Information

Chemical Name:4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide
CAS No.:871939-86-5
Molecular Formula:C₁₅H₁₅NO₂S
Molecular Weight:273.356
Hs Code.:

Synonyms:4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Suppliers and Price of 4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

There total 3 articles about 4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6873-55-8
p-tolylsulfinyl amide

: 591-31-1
3-methoxy-benzaldehyde

: 871939-86-5
4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; Heating;
DOI:10.1021/ol052250w

Reference yield:

: 103-19-5
di(p-tolyl) disulfide

: 871939-86-5
4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 100 percent / NBS / 20 °C

2.1: LiHMDS / tetrahydrofuran / -78 - 20 °C

2.2: 93 percent / NH₄Cl; H₂O / tetrahydrofuran / 1 h / 20 °C

3.1: 92 percent / Ti(OEt)4 / CH₂Cl₂ / Heating

With titanium(IV) tetraethanolate; N-Bromosuccinimide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol052250w

Reference yield:

: 672-78-6
methyl p-toluene sulfinate

: 871939-86-5
4-Methyl-benzenesulfinic acid 1-(3-methoxy-phenyl)-meth-(E)-ylideneamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiHMDS / tetrahydrofuran / -78 - 20 °C

1.2: 93 percent / NH₄Cl; H₂O / tetrahydrofuran / 1 h / 20 °C

2.1: 92 percent / Ti(OEt)4 / CH₂Cl₂ / Heating

With titanium(IV) tetraethanolate; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol052250w