3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide

Base Information

• Chemical Name: 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide
• CAS No.: 186186-65-2
• Molecular Formula: C₁₀H₁₄BrFO₅
• Molecular Weight: 313.121
• Mol file: 186186-65-2.mol

Synonyms:3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide

Chemical Property of 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide

There total 1 articles about 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide (186186-65-2) + (3,4-Di-O-acetyl-2-deoxy-2-fluoro-β-L-fucopyranosyl) dibenzyl phosphate (188783-82-6)

Guidance literature:

Reference yield: 92.0%

phosphoric acid dibenzyl ester (1623-08-1) + 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide (186186-65-2) → (3,4-Di-O-acetyl-2-deoxy-2-fluoro-β-L-fucopyranosyl) dibenzyl phosphate (188783-82-6)

Guidance literature:

With silver (II) carbonate; 3 A molecular sieve; In diethyl ether; dichloromethane; acetonitrile; for 21h; Ambient temperature;

DOI:10.1016/S0968-0896(96)00258-1

Reference yield: 89.0%

Ag2 CO3 + ? molecular sieves + phosphoric acid dibenzyl ester (1623-08-1) + 3,4-di-O-acetyl-2,6-dideoxy-2-fluoro-α-L-galactopyranosyl bromide (186186-65-2) → β-L-Fucopyranosyl phosphate (16562-59-7,28553-11-9)

Guidance literature:

In benzene;

Downstream raw materials:

(3,4-Di-O-acetyl-2-deoxy-2-fluoro-β-L-fucopyranosyl) dibenzyl phosphate

β-L-Fucopyranosyl phosphate