methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate

Base Information

Chemical Name:methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate
CAS No.:67059-93-2
Molecular Formula:C₂₀H₂₁ClO₄
Molecular Weight:360.837
Hs Code.:

Synonyms:methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate

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Chemical Property of methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate

Chemical Property:

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Technology Process of methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate

There total 3 articles about methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67059-92-1
6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylic acid chloride

: 67059-93-2
methyl 6-chloro-4-tert.-butyl-4-phenyl-[4H]-1,3-benzodioxin-2-carboxylate

Guidance literature:: With triethylamine; In methanol; benzene;

Reference yield:

: 85-19-8
(5-chloro-2-hydroxyphenyl)phenylmethanone

: 67059-93-2,86617-03-0
(2R,4R)-4-tert-Butyl-6-chloro-4-phenyl-4H-benzo[1,3]dioxine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: benzene; diethyl ether / 2 h / Heating

2: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

3: Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In 1,4-dioxane; diethyl ether; benzene;

Reference yield:

: 67059-91-0
5-chloro-α-tert.-butyl-2-hydroxy-α-phenyl-benzenemethanol

: 67059-93-2,86617-03-0
(2R,4R)-4-tert-Butyl-6-chloro-4-phenyl-4H-benzo[1,3]dioxine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

2: Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In 1,4-dioxane;