2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Base Information

Chemical Name:2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane
CAS No.:87450-96-2
Molecular Formula:C₁₉H₂₆NO₈P
Molecular Weight:427.391
Hs Code.:

Synonyms:2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

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Chemical Property of 2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Chemical Property:

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Technology Process of 2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

There total 7 articles about 2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4187-59-1,4187-60-4,27583-43-3,29569-80-0,51606-49-6,51606-50-9,69308-85-6,96553-66-1,106758-67-2
trans-2-hydroxymethylcyclohexanol

: 87450-96-2
12-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus oxychloride, pyridine / diethyl ether

2: pyridine / 24 h / 0 °C

With pyridine; trichlorophosphate; In pyridine; diethyl ether;
DOI:10.1021/ja00361a033

Reference yield:

: 4187-59-1,4187-60-4,27583-43-3,29569-80-0,51606-49-6,51606-50-9,69308-85-6,96553-66-1,106758-67-2
trans-2-hydroxymethylcyclohexanol

: 87450-96-2
12-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus oxychloride, pyridine / diethyl ether

2: pyridine / 24 h / 0 °C

With pyridine; trichlorophosphate; In pyridine; diethyl ether;
DOI:10.1021/ja00361a033

Reference yield:

: 4187-59-1,4187-60-4,27583-43-3,29569-80-0,51606-49-6,51606-50-9,69308-85-6,96553-66-1,106758-67-2
trans-2-hydroxymethylcyclohexanol

: 87450-96-2
2-(N-carbobenzoxy-L-serine methyl ester)-2-oxo-trans-5,6-tetramethylene-1,3,2-dioxaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus oxychloride, pyridine / diethyl ether

2: pyridine / 24 h / 0 °C

With pyridine; trichlorophosphate; In pyridine; diethyl ether;
DOI:10.1021/ja00361a033