6-(benzyloxy)-4-oxohexanal ethylene ketal

Base Information

Chemical Name:6-(benzyloxy)-4-oxohexanal ethylene ketal
CAS No.:122698-45-7
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

Synonyms:6-(benzyloxy)-4-oxohexanal ethylene ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(benzyloxy)-4-oxohexanal ethylene ketal

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Technology Process of 6-(benzyloxy)-4-oxohexanal ethylene ketal

There total 4 articles about 6-(benzyloxy)-4-oxohexanal ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122698-44-6
6-(benzyloxy)-4-oxohexanol ethylene ketal

: 122698-45-7
6-(benzyloxy)-4-oxohexanal ethylene ketal

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1.25h;
DOI:10.1021/jo00280a021

Reference yield:

: 156907-76-5
ethyl 2-<(trimethylsilyl)oxy>-2-vinylcyclopropane-1-carboxylate

: 122698-45-7
6-(benzyloxy)-4-oxohexanal ethylene ketal

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / potassium carbonate / 1.) 20 deg C, 8 h, 2.) 45 deg C, 8 h

2: p-toluenesulfonic acid / benzene / 5 h / Heating

3: 2.01 g / lithium aluminum hydride (LAH) / tetrahydrofuran / 4 h / 20 °C

4: PCC, sodium acetate / CH₂Cl₂ / 1.25 h / 20 °C

With lithium aluminium tetrahydride; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jo00280a021

Reference yield:

: 122698-25-3
ethyl 6-(benzyloxy)-4-oxohexanoate

: 122698-45-7
6-(benzyloxy)-4-oxohexanal ethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid / benzene / 5 h / Heating

2: 2.01 g / lithium aluminum hydride (LAH) / tetrahydrofuran / 4 h / 20 °C

3: PCC, sodium acetate / CH₂Cl₂ / 1.25 h / 20 °C

With lithium aluminium tetrahydride; sodium acetate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jo00280a021