Technology Process of C32H46N2O7
There total 4 articles about C32H46N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H17NO5;
With
2-chloro-1-methyl-pyridinium iodide; triethylamine;
In
dichloromethane;
for 0.25h;
Inert atmosphere;
Reflux;
C14H21NO3;
In
dichloromethane;
for 48h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tetlet.2011.05.004
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 70 °C
2.1: lithium hydroxide / tetrahydrofuran; water / 0 - 20 °C
2.2: 0 °C
3.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 0.25 h / Inert atmosphere; Reflux
3.2: 48 h / Inert atmosphere; Reflux
With
2-chloro-1-methyl-pyridinium iodide; potassium carbonate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.05.004
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 70 °C
2.1: lithium hydroxide / tetrahydrofuran; water / 0 - 20 °C
2.2: 0 °C
3.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 0.25 h / Inert atmosphere; Reflux
3.2: 48 h / Inert atmosphere; Reflux
With
2-chloro-1-methyl-pyridinium iodide; potassium carbonate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.05.004
