cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

Base Information

Chemical Name:cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen
CAS No.:18499-57-5
Molecular Formula:C₂₆H₁₆O₂
Molecular Weight:360.412
Hs Code.:

Synonyms:cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

Suppliers and Price of cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

There total 1 articles about cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 10486-08-5
sodium p-thiocresolate

: 932-87-6
1-Bromo-2-phenylacetylene

: 951165-87-0
(9s,10s)-9,10-diethynyl-9,10-dihydroanthracene-9,10-diol

: 932-87-6
1-Bromo-2-phenylacetylene

: C₂₂H₂₀S₂

: 18499-57-5
cis-10-(Phenylbutadiinyl)-9-ethinyl-cis-9,10-dihydroxy-9,10-dihydro-anthracen

Guidance literature:: With MeCo(CN)2Li; In tetrahydrofuran; for 18h; Product distribution; for -78 deg C to r.t., variation of reagent;
DOI:10.1055/s-1995-3872

Reference yield:

: 18499-57-5
trans-9-(Phenylbutadiinyl)-10-ethinyl-trans-9,10-dihydroxy-9,10-dihydro-anthracen

: 18499-65-5
1,1-diphenyl-3-(10-phenylbutadiynyl-[9]anthryl)-prop-2-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂, AcOH

2: KOH / tetrahydrofuran

With potassium hydroxide; acetic acid; tin(ll) chloride; In tetrahydrofuran;