(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

Base Information

Chemical Name:(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene
CAS No.:90056-26-1
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

Synonyms:(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

Chemical Property:

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Technology Process of (1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

There total 5 articles about (1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97691-01-5
C₂₁H₃₀O₃Se

: 90056-26-1
(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

Guidance literature:: With pyridine; In tetrachloromethane; for 0.5h; Yield given; Heating;
DOI:10.1021/jo00218a026

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 90056-26-1
(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: PPTS / CH₂Cl₂ / 16 h / Ambient temperature

2: pyridine, 15percent aq. H₂O₂ / CH₂Cl₂ / 1.5 h / Ambient temperature

3: pyridine / CCl₄ / 0.5 h / Heating

With pyridine; dihydrogen peroxide; pyridinium p-toluenesulfonate; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo00218a026

Reference yield:

: 76339-71-4
(2S,3R,5S)-2-methyl-5-(1-methylethenyl)-3-(phenylseleno)-cyclohexanone

: 90056-26-1
(1S,2R,5S)-2-methyl-5-(1-methylethenyl)-1-((tetrahydropyran-2-yl)oxy)-3-cyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / diisobutylaluminum hydride (DIBAH) / toluene / 3 h / -78 °C

2: PPTS / CH₂Cl₂ / 16 h / Ambient temperature

3: pyridine, 15percent aq. H₂O₂ / CH₂Cl₂ / 1.5 h / Ambient temperature

4: pyridine / CCl₄ / 0.5 h / Heating

With pyridine; dihydrogen peroxide; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In tetrachloromethane; dichloromethane; toluene;
DOI:10.1021/jo00218a026