C₃₁H₃₈FN₅O₄

Base Information

Chemical Name:C₃₁H₃₈FN₅O₄
CAS No.:1408065-33-7
Molecular Formula:C₃₁H₃₈FN₅O₄
Molecular Weight:563.672
Hs Code.:

C<sub>31</sub>H<sub>38</sub>FN<sub>5</sub>O<sub>4</sub>

Synonyms:C₃₁H₃₈FN₅O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₈FN₅O₄

Chemical Property:

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Technology Process of C₃₁H₃₈FN₅O₄

There total 6 articles about C₃₁H₃₈FN₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1408065-31-5
C₃₅H₄₆FN₅O₄

: 1408065-33-7
C₃₁H₃₈FN₅O₄

Guidance literature:: With silica gel; In toluene; for 6h; Inert atmosphere; Reflux;
DOI:10.1039/c2ob26103k

Reference yield:

: 63128-51-8
5-(tert-butoxy)-5-oxopentanoic acid

: 1408065-33-7
C₃₁H₃₈FN₅O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 28 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: manganese(IV) oxide / dichloromethane / 22 h / 20 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 18 h / 20 °C / Inert atmosphere

5.1: silica gel / toluene / 6 h / Inert atmosphere; Reflux

With manganese(IV) oxide; tetrabutyl ammonium fluoride; silica gel; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1039/c2ob26103k

Reference yield:

: 1408065-78-0
Fmoc-Glu-OtBu

: 1408065-33-7
C₃₁H₃₈FN₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: manganese(IV) oxide / dichloromethane / 22 h / 20 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 18 h / 20 °C / Inert atmosphere

4: silica gel / toluene / 6 h / Inert atmosphere; Reflux

With manganese(IV) oxide; tetrabutyl ammonium fluoride; silica gel; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1039/c2ob26103k