1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane

Base Information

• Chemical Name: 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane
• CAS No.: 749923-77-1
• Molecular Formula: C₂₄H₃₂N₄O₂
• Molecular Weight: 408.544
• Mol file: 749923-77-1.mol

Synonyms:1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane

Chemical Property of 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane

There total 2 articles about 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

ethyl (E)-4-phenylbut-3-enoate (1205-84-1) + Trimethylenediamine (109-76-2,54018-94-9) → 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane (749923-77-1)

Guidance literature:

With hydrogenchloride; In ethanol; for 12h; Heating;

DOI:10.1016/j.saa.2003.12.016

Reference yield:

ethyl 3-phenyl-2-propenoate (103-36-6) + Trimethylenediamine (109-76-2,54018-94-9) → 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane (749923-77-1)

Guidance literature:

With hydrogenchloride; In ethanol; at 80 ℃;

DOI:10.1080/00958972.2010.510557

Reference yield:

vanadyl(IV) sulphate pentahydrate + 1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane (749923-77-1) → [VO(1,5,9,13-tetraaza-2,10-dioxo-4,12-diphenylcyclohexadecane)]SO4

Guidance literature:

With (C₂H₅)3N; In ethanol; to hot soln. of tetraazamacrocyclic ligand in EtOH hot soln. of VOSO4*5H2O in EtOH and few drops of Et3N were added, refluxed for 2 h; filtered, washed with cold EtOH, dried in vac., elem. anal.;

DOI:10.1016/j.ica.2008.09.043

upstream raw materials:

ethyl (E)-4-phenylbut-3-enoate

Trimethylenediamine

ethyl 3-phenyl-2-propenoate