11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

Base Information

Chemical Name:11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin
CAS No.:167256-57-7
Molecular Formula:C₄₃H₅₄O₁₇
Molecular Weight:842.892
Hs Code.:

Synonyms:11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

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Technology Process of 11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

There total 3 articles about 11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 167256-58-8
11-benzyloxy-22,23-dihydro-23-β-methoxy-7-oxoazadirachtin

: 167256-57-7
11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at 0 ℃;
DOI:10.1002/anie.200703028

Reference yield: 43.0%

: 167256-58-8
11-benzyloxy-22,23-dihydro-23-β-methoxy-7-oxoazadirachtin

: 167256-57-7
11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

: <7R> 11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at -5 - 0 ℃; for 4h;
DOI:10.1016/0040-4020(95)00297-L

Reference yield:

: 11-benzyloxy-22-α-bromo-22,23-dihydro-23-methoxyazadirachtin

: 11-benzyloxy-22,23-dihydro-23-α-methoxyazadirachtin

: 167256-57-7
11-benzyloxy-22,23-dihydro-23-β-methoxyazadirachtin

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 0.666667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0040-4020(95)00297-L