3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole

Base Information

• Chemical Name: 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole
• CAS No.: 116967-31-8
• Molecular Formula: C₁₈H₁₄N₂S₄
• Molecular Weight: 386.587
• Mol file: 116967-31-8.mol

Synonyms:3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole

Chemical Property of 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole

There total 4 articles about 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3H,6H-2,5-bis(p-methyl-phenyl)-1,2-thiazolino<5,4-d>1,2-thiazoline-3,6-dithione (116967-38-5) → 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole (116967-31-8)

Guidance literature:

With mercury(II) diacetate; In acetic acid; for 0.5h; Ambient temperature;

DOI:10.1016/0040-4020(89)80039-0

Reference yield: 80.0%

p-toluidine (106-49-0,12221-03-3) + 3H,6H-3,6-bismethylthio-1,2-dithiolo<4,3-c>1,2-dithiolium tetrafluoroborate → 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole (116967-31-8)

Guidance literature:

With acetic acid; for 0.5h; Heating;

DOI:10.1016/0040-4020(89)80039-0

Reference yield: 12.0%

3H,6H-<1,2>dithiolo<4,3-c><1,2>dithiole-3,6-dithione (56423-74-6) + p-toluidine (106-49-0,12221-03-3) → 3H,6H-3-p-methyl-phenylimino-1,2-dithiolo<4,3-c>1,2-dithiole-6-thione (116967-35-2) + 3H,6H-2,5-bis(p-methyl-phenyl)-1,2-thiazolino<5,4-d>1,2-thiazoline-3,6-dithione (116967-38-5) + 3H,6H-3,6-bis(p-methyl-phenylimino)-1,2-dithiolo<4,3-c>1,2-dithiole (116967-31-8)

Guidance literature:

In toluene; for 12h; Heating;

DOI:10.1016/0040-4020(89)80039-0

upstream raw materials:

3H,6H-<1,2>dithiolo<4,3-c><1,2>dithiole-3,6-dithione

p-toluidine

3H,6H-2,5-bis(p-methyl-phenyl)-1,2-thiazolino<5,4-d>1,2-thiazoline-3,6-dithione

Downstream raw materials:

3H,6H-2,5-bis(p-methyl-phenyl)-1,2-thiazolino<5,4-d>1,2-thiazoline-3,6-dithione