Technology Process of C37H33N3O6
There total 6 articles about C37H33N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 90 ℃;
for 17h;
DOI:10.1016/j.bmcl.2013.06.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / 48 h / 0 °C
1.2: 1 h
2.1: water; lithium hydroxide / tetrahydrofuran / 20 °C
3.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
4.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C
5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C
With
hydrogenchloride; water; caesium carbonate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
2: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C
With
caesium carbonate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027