AE-641/15124054

Base Information

• Chemical Name: AE-641/15124054
• CAS No.: 380638-21-1
• Molecular Formula: C₁₈H₁₇N₃O₃S
• Molecular Weight: 355.417

Synonyms:AE-641/15124054

Chemical Property of AE-641/15124054

Chemical Property:

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Technology Process of AE-641/15124054

There total 2 articles about AE-641/15124054 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-[5-acetyl-3-cyano-4-(4-methoxy-phenyl)-6-methyl-pyridin-2-ylsulfanyl]-acetamide (470455-86-8) → AE-641/15124054 (380638-21-1)

Guidance literature:

With sodium ethanolate; In ethanol; for 0.333333h; Heating;

DOI:10.1002/jccs.200200035

Reference yield:

5-acetyl-3-cyano-4-(4-methoxyphenyl)-6-methylpyridine-2(1H)-thione (121104-38-9) → AE-641/15124054 (380638-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / CH₃CO₂Na*3H₂O / ethanol / 2 h / Heating

2: 91 percent / NaOEt / ethanol / 0.33 h / Heating

With sodium ethanolate; sodium acetate; In ethanol;

DOI:10.1002/jccs.200200035

Reference yield: 94.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + AE-641/15124054 (380638-21-1) → C24H25N3O3S

Guidance literature:

With acetic acid; for 3h; Heating;

DOI:10.1080/10426500490422155

upstream raw materials:

2-[5-acetyl-3-cyano-4-(4-methoxy-phenyl)-6-methyl-pyridin-2-ylsulfanyl]-acetamide

5-acetyl-3-cyano-4-(4-methoxyphenyl)-6-methylpyridine-2(1H)-thione

Downstream raw materials:

8-acetyl-9-(4'-methoxyphenyl)-2,7-dimethylpyrido[3',2':4,5]thieno[3,2-d]pyrimidin-4(3H)-one

8-Acetyl-9-(4-methoxy-phenyl)-7-methyl-3H-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-4-one

8-Acetyl-9-(4-methoxy-phenyl)-7-methyl-3H-pyrido[3',2':4,5]thieno[3,2-d][1,2,3]triazin-4-one

1-[4-Chloro-9-(4-methoxy-phenyl)-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

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