(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

Base Information

Chemical Name:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester
CAS No.:73233-07-5
Molecular Formula:C₂₂H₂₇F₃O₃S₂
Molecular Weight:460.582
Hs Code.:

Synonyms:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

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Technology Process of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

There total 2 articles about (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 42723-32-0,42723-33-1,42723-34-2,79839-56-8
l-3-(2-methyl-4-oxo-2-cyclohexenyl)propanol ethylene thioketal

: 73233-07-5
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

Guidance literature:: With pyridine; 1-amino-3-(dimethylamino)propane; In tetrachloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1021/ja00521a057

Reference yield:

: 42723-28-4,42723-30-8,42723-31-9
3-(7-Methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propionic acid

: 73233-07-5
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid 3-(7-methyl-1,4-dithia-spiro[4.5]dec-6-en-8-yl)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium bis(2-methoxyethoxy)alumino hydride / tetrahydrofuran; benzene / 4 h / 0 °C

2: 90 percent / pyridine, 3-dimethylamino-1-aminopropane / CCl₄ / 0.08 h / Ambient temperature

With pyridine; 1-amino-3-(dimethylamino)propane; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; tetrachloromethane; benzene;
DOI:10.1021/ja00521a057