1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

Base Information

Chemical Name:1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol
CAS No.:603126-53-0
Molecular Formula:C₃₂H₃₆O₁₂
Molecular Weight:612.631
Hs Code.:

Synonyms:1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

Chemical Property:

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Technology Process of 1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

There total 4 articles about 1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 51019-44-4
(S)-2-chloro-2-oxo-1-phenylethyl acetate

: 51548-88-0,96039-15-5,98974-89-1,128110-25-8
(+/-)-1,2:4,5-di-O-isopropylidene-myo-inositol

: 191488-25-2
D-3,6-di-O-[(S)-O-acetylmandeloyl]-1,2:4,5-di-O-isopropylidene-myo-inositol

: 603126-53-0
1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/S0957-4166(03)00402-6 DOI:10.1016/j.tetasy.2004.11.030

Reference yield: 18.0%

: 7322-88-5
(S)-acetylmandelic acid

: 51548-88-0,96039-15-5,98974-89-1,128110-25-8
(+/-)-1,2:4,5-di-O-isopropylidene-myo-inositol

: 191488-25-2
D-3,6-di-O-[(S)-O-acetylmandeloyl]-1,2:4,5-di-O-isopropylidene-myo-inositol

: 603126-53-0
1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/a608337d

Reference yield:

: 7322-88-5
(S)-acetylmandelic acid

: 603126-53-0
1D-1,4-di-O-[(S)-O-acetylmandeloyl]-2,3:5,6-di-O-isopropylidene-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 0.25 h / 0 °C

2: 42 percent / pyridine / CH₂Cl₂ / 3 h / 0 - 20 °C

With pyridine; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.11.030